ZHENGZHOU HENGTONG FURNACE CO,. LTD
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7 kW Melt-spinning System with the Glove Box
7 kW Melt-spinning System with the Glove Box
  • 7 kW Melt-spinning System with the Glove Box
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SPECIFICATIONS:

Features

7 kW induction heater to melt alloy with ease.

10 - 20g samples up to 1600°C

Ø200mm copper flywheel with max. 31 m/s spinning speed

Adjustable distance between crucible and copper wheel. 0~10mm manually

One sample transfer tank is included to prevent samples from exposure to air during sample loading

Two systems can be isolated by an ISO160-K gate valve to prevent cross-contamination during melt-spinning

Power

208- 240VAC, single phase, 50/60 Hz, 7kW for melt-spinning system

110VAc or 208-240 VAC, single phase, 50/60 Hz, 1.5 kW for the glove box.

Total 8.5 KW.   Calbe inclided , but no plug

Vacuum Chamber

Stainless steel vacuum chamber: 300 x 300 x 480 mm

Hinged door with quartz observation window (120mm dia.)

Vacuum level: 5e-5 torr within 30 minutes by turbopump

KF40 and ISO100-K vacuum port is built to the chamber.

Induction Heater

Induction Heater:

Desktop 7KW Induction Heater, 30 - 80kHz (Standard, non-adjustable frequency)

High Frequency 10 KW Induction Heater, 80 - 200kHz (available at extra cost)

Max. sample load: 5 - 20g (Fe based )

Max. working temperature: 2000°C

Temperature control of the melt-spinning is not available.

Induction coils with different sizes is available upon request.

Water cooling is required for the induction heater.

Crucibles

Two quartz crucibles with an orifice of 0.5 - 1mm dia. are included for materials of melting point < 1200ºC

Customized crucibles made of quartz or BN are available upon request at extra cost

Optional graphite sheath (graphite casing+quartz insulation+larger induction coil in diameter) are also available upon request at extra cost for refractory and low magnetic permeability materials

Spinning Wheel

Copper flywheel without water cooling (200 mm Dia. x 40 mm W)

0 - 31 m/s adjustable

Max. Speed: 3000 RPM

Max. Ribbon width: 12 mm (depended on the nozzle of crucible)

The water-cooling wheel/stainless steel wheel is available upon request with extra cost

Collection Tube

Spun and solidified material is collected by the vacuum-sealed drum.

Collector Length: 300 mm

Glove Box Chamber

Case Material: Stainless steel 304 with 3 mm thickness

Chamber dimension: 1200 mm L x 740 mm W x 900 mm H

Openable front window panel (tempered glass, 8 mm thick)

Chamber Condition

Automatic regeneration for the purification column

Automatic purging function to quickly bring O2 < 100ppm & H2O < 50 ppm before purifying.

Automatic pressure control to keep the pressure at a constant level.

Water <1 ppm (20 °C, 1 atm)

Oxygen <1 ppm (20 °C, 1 atm)

Leak Rate

<0.05 vol% / hr (depending on oxygen concentration inside the glove box)

Antechamber

Main antechamber Ø360 × 600 L in mm

Second antechamber Ø150 × 220 L in mm

Working Gas

Operating gas: Inert gas such as N2, Ar, He

Regenerating gas: 5% H2 blended inert gas

Gas Purification System

Automated regeneration process

Automated Water and oxygen purification

Purification cylinder: BASF R3-11 Copper Catalyst and Lindy Molecular Sieve

Pipeline: 304 stainless steel, KF40, and KF25 ports

Ports & Fittings

Total three KF40 ports on the back of the glove box

Gas Filter

Inlet and outlet HEPA filter can eliminate particle size > 0.3 μm

Carbon and solvent vapor filters are available upon request at the extra cost for flammable vapor

Pressure Control System

Automatic pressure control by PLC for the Glove Box Chamber

Pressure range: +/- 12 mbar

Manual pressure control is allowed via a foot pedal

Purging System

An automatic purging system allows easy operating and reduces gas consumption

Control System

Siemens PLC control system with 7" touchscreen display

Water concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

Oxygen concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

Pressure: -12 to 12 mbar with an accuracy of 0.1 mbar

Records for total hours of operation, total regeneration times, time since last regeneration

Pump

240 L/m heavy-duty double stage rotary vane pump is included for glove box.

Gloves

A pair of 9 3/4" butyl gloves is included for immediate use

Optional

A water-chiller is required but not included

A separate pumping system is required for melt-spinning but not included.

Warranty

One-year limited warranty with lifetime support

During melt-spinning, metal ingots are melted via induction heating and propelled by pressurized inert gas. A thin stream of the melt is cast onto a spinning copper drum. The rapid quenching and solidification process enables the alloy forms amorphous ribbons in a few seconds.


SPECIFICATIONS:

Features

7 kW induction heater to melt alloy with ease.

10 - 20g samples up to 1600°C

Ø200mm copper flywheel with max. 31 m/s spinning speed

Adjustable distance between crucible and copper wheel. 0~10mm manually

One sample transfer tank is included to prevent samples from exposure to air during sample loading

Two systems can be isolated by an ISO160-K gate valve to prevent cross-contamination during melt-spinning

Power

208- 240VAC, single phase, 50/60 Hz, 7kW for melt-spinning system

110VAc or 208-240 VAC, single phase, 50/60 Hz, 1.5 kW for the glove box.

Total 8.5 KW.   Calbe inclided , but no plug

Vacuum Chamber

Stainless steel vacuum chamber: 300 x 300 x 480 mm

Hinged door with quartz observation window (120mm dia.)

Vacuum level: 5e-5 torr within 30 minutes by turbopump

KF40 and ISO100-K vacuum port is built to the chamber.

Induction Heater

Induction Heater:

Desktop 7KW Induction Heater, 30 - 80kHz (Standard, non-adjustable frequency)

High Frequency 10 KW Induction Heater, 80 - 200kHz (available at extra cost)

Max. sample load: 5 - 20g (Fe based )

Max. working temperature: 2000°C

Temperature control of the melt-spinning is not available.

Induction coils with different sizes is available upon request.

Water cooling is required for the induction heater.

Crucibles

Two quartz crucibles with an orifice of 0.5 - 1mm dia. are included for materials of melting point < 1200ºC

Customized crucibles made of quartz or BN are available upon request at extra cost

Optional graphite sheath (graphite casing+quartz insulation+larger induction coil in diameter) are also available upon request at extra cost for refractory and low magnetic permeability materials

Spinning Wheel

Copper flywheel without water cooling (200 mm Dia. x 40 mm W)

0 - 31 m/s adjustable

Max. Speed: 3000 RPM

Max. Ribbon width: 12 mm (depended on the nozzle of crucible)

The water-cooling wheel/stainless steel wheel is available upon request with extra cost

Collection Tube

Spun and solidified material is collected by the vacuum-sealed drum.

Collector Length: 300 mm

Glove Box Chamber

Case Material: Stainless steel 304 with 3 mm thickness

Chamber dimension: 1200 mm L x 740 mm W x 900 mm H

Openable front window panel (tempered glass, 8 mm thick)

Chamber Condition

Automatic regeneration for the purification column

Automatic purging function to quickly bring O2 < 100ppm & H2O < 50 ppm before purifying.

Automatic pressure control to keep the pressure at a constant level.

Water <1 ppm (20 °C, 1 atm)

Oxygen <1 ppm (20 °C, 1 atm)

Leak Rate

<0.05 vol% / hr (depending on oxygen concentration inside the glove box)

Antechamber

Main antechamber Ø360 × 600 L in mm

Second antechamber Ø150 × 220 L in mm

Working Gas

Operating gas: Inert gas such as N2, Ar, He

Regenerating gas: 5% H2 blended inert gas

Gas Purification System

Automated regeneration process

Automated Water and oxygen purification

Purification cylinder: BASF R3-11 Copper Catalyst and Lindy Molecular Sieve

Pipeline: 304 stainless steel, KF40, and KF25 ports

Ports & Fittings

Total three KF40 ports on the back of the glove box

Gas Filter

Inlet and outlet HEPA filter can eliminate particle size > 0.3 μm

Carbon and solvent vapor filters are available upon request at the extra cost for flammable vapor

Pressure Control System

Automatic pressure control by PLC for the Glove Box Chamber

Pressure range: +/- 12 mbar

Manual pressure control is allowed via a foot pedal

Purging System

An automatic purging system allows easy operating and reduces gas consumption

Control System

Siemens PLC control system with 7" touchscreen display

Water concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

Oxygen concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

Pressure: -12 to 12 mbar with an accuracy of 0.1 mbar

Records for total hours of operation, total regeneration times, time since last regeneration

Pump

240 L/m heavy-duty double stage rotary vane pump is included for glove box.

Gloves

A pair of 9 3/4" butyl gloves is included for immediate use

Optional

A water-chiller is required but not included

A separate pumping system is required for melt-spinning but not included.

Warranty

One-year limited warranty with lifetime support

During melt-spinning, metal ingots are melted via induction heating and propelled by pressurized inert gas. A thin stream of the melt is cast onto a spinning copper drum. The rapid quenching and solidification process enables the alloy forms amorphous ribbons in a few seconds.