ZHENGZHOU HENGTONG FURNACE CO,. LTD
7 kW Melt-spinning System with the Glove Box
  • 7 kW Melt-spinning System with the Glove Box
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7 kW Melt-spinning System with the Glove Box

HT-200S is a benchtop vacuum melt spinning system for preparing amorphous metallic ribbons up to 2000℃. Air-sensitive samples can be prepared inside the glove box and transferred to the melt-spinning system without exposure to the air via a transfer tank. With a direct couple with the glove box, the sample collection process can also be completed inside a glove box.

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  • Product Details
  • SPECIFICATIONS:

    Features

    l 7 kW induction heater to melt alloy with ease.

    l 10 - 20g samples up to 1600°C

    l Ø200mm copper flywheel with max. 31 m/s spinning speed

    l Adjustable distance between crucible and copper wheel. 0~10mm manually

    l One sample transfer tank is included to prevent samples from exposure to air during sample loading

    l Two systems can be isolated by an ISO160-K gate valve to prevent cross-contamination during melt-spinning

    Power

    l 208- 240VAC, single phase, 50/60 Hz, 7kW for melt-spinning system

    l 110VAc or 208-240 VAC, single phase, 50/60 Hz, 1.5 kW for the glove box.

    l Total 8.5 KW.   Calbe inclided , but no plug

    Vacuum Chamber

    l Stainless steel vacuum chamber: 300 x 300 x 480 mm

    l Hinged door with quartz observation window (120mm dia.)

    l Vacuum level: 5e-5 torr within 30 minutes by turbopump

    l KF40 and ISO100-K vacuum port is built to the chamber.

    Induction Heater

    l Induction Heater:

    l Desktop 7KW Induction Heater, 30 - 80kHz (Standard, non-adjustable frequency)

    l High Frequency 10 KW Induction Heater, 80 - 200kHz (available at extra cost)

    l Max. sample load: 5 - 20g (Fe based )

    l Max. working temperature: 2000°C

    l Temperature control of the melt-spinning is not available.

    l Induction coils with different sizes is available upon request.

    l Water cooling is required for the induction heater.

    Crucibles

    l Two quartz crucibles with an orifice of 0.5 - 1mm dia. are included for materials of melting point < 1200ºC

    l Customized crucibles made of quartz or BN are available upon request at extra cost

    l Optional graphite sheath (graphite casing+quartz insulation+larger induction coil in diameter) are also available upon request at extra cost for refractory and low magnetic permeability materials

    Spinning Wheel

    l Copper flywheel without water cooling (200 mm Dia. x 40 mm W)

    l 0 - 31 m/s adjustable

    l Max. Speed: 3000 RPM

    l Max. Ribbon width: 12 mm (depended on the nozzle of crucible)

    l The water-cooling wheel/stainless steel wheel is available upon request with extra cost

    Collection Tube

    l Spun and solidified material is collected by the vacuum-sealed drum.

    l Collector Length: 300 mm

    Glove Box Chamber

    l Case Material: Stainless steel 304 with 3 mm thickness

    l Chamber dimension: 1200 mm L x 740 mm W x 900 mm H

    l Openable front window panel (tempered glass, 8 mm thick)

    Chamber Condition

    l Automatic regeneration for the purification column

    l Automatic purging function to quickly bring O2 < 100ppm & H2O < 50 ppm before purifying.

    l Automatic pressure control to keep the pressure at a constant level.

    l Water <1 ppm (20 °C, 1 atm)

    l Oxygen <1 ppm (20 °C, 1 atm)

    Leak Rate

    l <0.05 vol% / hr (depending on oxygen concentration inside the glove box)

    Antechamber

    l Main antechamber Ø360 × 600 L in mm

    l Second antechamber Ø150 × 220 L in mm

    Working Gas

    l Operating gas: Inert gas such as N2, Ar, He

    l Regenerating gas: 5% H2 blended inert gas

    Gas Purification System

    l Automated regeneration process

    l Automated Water and oxygen purification

    l Purification cylinder: BASF R3-11 Copper Catalyst and Lindy Molecular Sieve

    l Pipeline: 304 stainless steel, KF40, and KF25 ports

    Ports & Fittings

    l Total three KF40 ports on the back of the glove box

    Gas Filter

    l Inlet and outlet HEPA filter can eliminate particle size > 0.3 μm

    l Carbon and solvent vapor filters are available upon request at the extra cost for flammable vapor

    Pressure Control System

    l Automatic pressure control by PLC for the Glove Box Chamber

    l Pressure range: +/- 12 mbar

    l Manual pressure control is allowed via a foot pedal

    Purging System

    l An automatic purging system allows easy operating and reduces gas consumption

    Control System

    l Siemens PLC control system with 7" touchscreen display

    l Water concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

    l Oxygen concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

    l Pressure: -12 to 12 mbar with an accuracy of 0.1 mbar

    l Records for total hours of operation, total regeneration times, time since last regeneration

    Pump

    l 240 L/m heavy-duty double stage rotary vane pump is included for glove box.

    Gloves

    l A pair of 9 3/4" butyl gloves is included for immediate use

    Optional

    l A water-chiller is required but not included

    l A separate pumping system is required for melt-spinning but not included.

    Warranty

    l One-year limited warranty with lifetime support

    During melt-spinning, metal ingots are melted via induction heating and propelled by pressurized inert gas. A thin stream of the melt is cast onto a spinning copper drum. The rapid quenching and solidification process enables the alloy forms amorphous ribbons in a few seconds.


    SPECIFICATIONS:

    Features

    l 7 kW induction heater to melt alloy with ease.

    l 10 - 20g samples up to 1600°C

    l Ø200mm copper flywheel with max. 31 m/s spinning speed

    l Adjustable distance between crucible and copper wheel. 0~10mm manually

    l One sample transfer tank is included to prevent samples from exposure to air during sample loading

    l Two systems can be isolated by an ISO160-K gate valve to prevent cross-contamination during melt-spinning

    Power

    l 208- 240VAC, single phase, 50/60 Hz, 7kW for melt-spinning system

    l 110VAc or 208-240 VAC, single phase, 50/60 Hz, 1.5 kW for the glove box.

    l Total 8.5 KW.   Calbe inclided , but no plug

    Vacuum Chamber

    l Stainless steel vacuum chamber: 300 x 300 x 480 mm

    l Hinged door with quartz observation window (120mm dia.)

    l Vacuum level: 5e-5 torr within 30 minutes by turbopump

    l KF40 and ISO100-K vacuum port is built to the chamber.

    Induction Heater

    l Induction Heater:

    l Desktop 7KW Induction Heater, 30 - 80kHz (Standard, non-adjustable frequency)

    l High Frequency 10 KW Induction Heater, 80 - 200kHz (available at extra cost)

    l Max. sample load: 5 - 20g (Fe based )

    l Max. working temperature: 2000°C

    l Temperature control of the melt-spinning is not available.

    l Induction coils with different sizes is available upon request.

    l Water cooling is required for the induction heater.

    Crucibles

    l Two quartz crucibles with an orifice of 0.5 - 1mm dia. are included for materials of melting point < 1200ºC

    l Customized crucibles made of quartz or BN are available upon request at extra cost

    l Optional graphite sheath (graphite casing+quartz insulation+larger induction coil in diameter) are also available upon request at extra cost for refractory and low magnetic permeability materials

    Spinning Wheel

    l Copper flywheel without water cooling (200 mm Dia. x 40 mm W)

    l 0 - 31 m/s adjustable

    l Max. Speed: 3000 RPM

    l Max. Ribbon width: 12 mm (depended on the nozzle of crucible)

    l The water-cooling wheel/stainless steel wheel is available upon request with extra cost

    Collection Tube

    l Spun and solidified material is collected by the vacuum-sealed drum.

    l Collector Length: 300 mm

    Glove Box Chamber

    l Case Material: Stainless steel 304 with 3 mm thickness

    l Chamber dimension: 1200 mm L x 740 mm W x 900 mm H

    l Openable front window panel (tempered glass, 8 mm thick)

    Chamber Condition

    l Automatic regeneration for the purification column

    l Automatic purging function to quickly bring O2 < 100ppm & H2O < 50 ppm before purifying.

    l Automatic pressure control to keep the pressure at a constant level.

    l Water <1 ppm (20 °C, 1 atm)

    l Oxygen <1 ppm (20 °C, 1 atm)

    Leak Rate

    l <0.05 vol% / hr (depending on oxygen concentration inside the glove box)

    Antechamber

    l Main antechamber Ø360 × 600 L in mm

    l Second antechamber Ø150 × 220 L in mm

    Working Gas

    l Operating gas: Inert gas such as N2, Ar, He

    l Regenerating gas: 5% H2 blended inert gas

    Gas Purification System

    l Automated regeneration process

    l Automated Water and oxygen purification

    l Purification cylinder: BASF R3-11 Copper Catalyst and Lindy Molecular Sieve

    l Pipeline: 304 stainless steel, KF40, and KF25 ports

    Ports & Fittings

    l Total three KF40 ports on the back of the glove box

    Gas Filter

    l Inlet and outlet HEPA filter can eliminate particle size > 0.3 μm

    l Carbon and solvent vapor filters are available upon request at the extra cost for flammable vapor

    Pressure Control System

    l Automatic pressure control by PLC for the Glove Box Chamber

    l Pressure range: +/- 12 mbar

    l Manual pressure control is allowed via a foot pedal

    Purging System

    l An automatic purging system allows easy operating and reduces gas consumption

    Control System

    l Siemens PLC control system with 7" touchscreen display

    l Water concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

    l Oxygen concentration: 0 - 1000 ppm with an accuracy of 0.1 ppm

    l Pressure: -12 to 12 mbar with an accuracy of 0.1 mbar

    l Records for total hours of operation, total regeneration times, time since last regeneration

    Pump

    l 240 L/m heavy-duty double stage rotary vane pump is included for glove box.

    Gloves

    l A pair of 9 3/4" butyl gloves is included for immediate use

    Optional

    l A water-chiller is required but not included

    l A separate pumping system is required for melt-spinning but not included.

    Warranty

    l One-year limited warranty with lifetime support

    During melt-spinning, metal ingots are melted via induction heating and propelled by pressurized inert gas. A thin stream of the melt is cast onto a spinning copper drum. The rapid quenching and solidification process enables the alloy forms amorphous ribbons in a few seconds.