ZHENGZHOU HENGTONG FURNACE CO,. LTD
Tube Furnace with Solid Precursor Sublimator for CVD 2D Layers of TMDs
  • Tube Furnace with Solid Precursor Sublimator for CVD 2D Layers of TMDs
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Tube Furnace with Solid Precursor Sublimator for CVD 2D Layers of TMDs

HTTF-1200-NW laboratory furnace is a compact 1100°C CVD tube furnace with a precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition.

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  • Product Details
  • HTTF-1200-NW laboratory furnace is a compact 1100°C CVD tube furnace with a precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition. The sample holder fixture mounted on the right flange is slidable for easy sample loading/unloading. Such a system configuration is suitable for growing a wide range of transitional metal dichalcogenides (TMD) such as MoSe2, MoS2. and wide bandgap semiconductors (such as h-BN) layers on substrate up to 3" diameter.

     

    Furnace and Preheater

    Compact CVD furnace system with:

    OD 110 xID 103 x L 740, mm Length quartz tube

    1100ºC Max. working temperature with +/- 1oC accuracy

    The water cooling flange on the right side is slidable for easy sample loading

    The water cooling flange on the left side between the heater and furnace is used for pre-heated gas input and sealing

    Four-channel gas inlet (1/8" Dia tube and tube fitting) are built-in on the left side flange

    One small heater is attached to the left side flange of the furnace to preheat input gas, liquid, or evaporate solid chemical, which will be then delivered to the CVD furnace:

    Please click the picture left for more details:

    1.2''O.D x 6''L SS tube as the heating chamber

    Vacuum sealed 1" ID small quartz tube inside the heater

    400ºC Max. working temperature (1000ºC heater is available upon request)

    The flange on the left side is for gas sealing and input

    Rated Voltage

    Single Phase, 208-240 VAC, 50/60 Hz, AWG 8# Power cord is included (without plug)

    Power consumption

    Max. 3600 W (20 A breaker required)

    Heating Zone

    CVD Furnace:  440 mm

    Constant temperature zone: 100 mm 

    Gas Heater:     150mm

    Working Temperature

    CVD Furnace:

    Max heating temperature: 1100°C (< 2 hour)

    Continuous working temperature: 200~1000°C

    Max heating & cooling rate: 20°C/min

    Heater:

    Continuous working temperature: RT~600°C

    Max heating & cooling rate: 20°C/min

    Temperature Control

    CVD Furnace and Heater (separate temp control):

    Digital controllers with PID/self-tuning functions and 30 segments programmable

    Thermocouple: K-type thermocouples, at the right side flange through feedthrough to control furnace temperature.

    Control accuracy: +/- 1°C

    RS485 Communications Port

    Vacuum

    and Gas Sealing & Flange

    The right flange of the CVD furnace

    Water cooling flanges to prevent sealing o-ring from melting

    KF25 vacuum port to a pump

    Slidable for the customer to easily and fast push/pull in/out a sample

    One quartz wafer holder (3" Dia) is included and the flange with heating radiation block

    An anti-corrosive capacitance diaphragm gauge is included

    Left flange (between CVD Furnace and Heater) with four 1/8'' Swagelok fittings for 1/8'' tube:

    Two 1/8'' fitting on the flange for independently and directly delivering any gas into the CVD furnace

    One 1/8'' fitting for delivering heated gas from heater to CVD furnace

    One 1/4'' fitting for bypassing the gas (without heating) to the CVD furnace (inside the CVD furnace, the gas tube is merged with the heated gas pipe by a T fitting)

    Note: How gas pipe assembled in the CVD furnace through above 1/8'' fitting:

    One 1/4'' quartz tube delivers the vapor gas from the heater (also the bypass gas by a T fitting)

    Two 1/4'' quartz tube delivery extra gas via the two separate 1/8'' fitting on the big furnace left the flange

    These three 1/4'' quartz tubes inside the CVD furnace are in parallel and vertically 1'' higher than the sample holder

    These three 1/4'' quartz tubes can be easily removed to clean or replaced once get stuck or corroded

    The optional Liquid Injection device-optional

    For direct liquid CVD  ( DLCVD), you may consider the below devices for liquid injection:

    Net weight

    110kg

    Dimensions

    Standard:    62"L X 18"W X 23"H

    Maximum:   80"L X 18"W X 32"H  (Lid open and right-side flange slide out)

    Shipping Weight & Dimensions

    380 lbs

    48"x40"x54"

    Warranty

    One-year limited warranty for electrical parts. (Consumable parts such as processing tubes, o-rings and etc are not covered by the warranty)

    You may order a replacement quartz tube here:

    Laptop, software & WiFi Control (Optional)

    Brand new laptop with Microsoft Windows 10 

    Labview Based Temperature Control System enables the user to edit temperature profiles, manage heat-treatment recipes, record, and plot data for MTI furnaces.

    A wireless remote control provides up to 300 meters of operating range.

    Eurotherm temperature controller with software is available upon request at extra cost, which can provide +/- 0.1oC accuracy. ( see product options bar)

    Warning

    The tube furnaces with quartz tubes are designed for use under vacuum and low pressure <0.2 bars (relative to 1 atm, absolute pressure = 1.2 bar if used in air)

    Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. 

    Vacuum pressures may only be safely used up to 1000°C 

     

    CVD Chemical Vapor Deposition furnaces is a process which allows the creation of a deposit on the surface of mechanical parts, to protect them from oxidation and corrosion.


    HTTF-1200-NW laboratory furnace is a compact 1100°C CVD tube furnace with a precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition. The sample holder fixture mounted on the right flange is slidable for easy sample loading/unloading. Such a system configuration is suitable for growing a wide range of transitional metal dichalcogenides (TMD) such as MoSe2, MoS2. and wide bandgap semiconductors (such as h-BN) layers on substrate up to 3" diameter.

     

    Furnace and Preheater

    Compact CVD furnace system with:

    OD 110 xID 103 x L 740, mm Length quartz tube

    1100ºC Max. working temperature with +/- 1oC accuracy

    The water cooling flange on the right side is slidable for easy sample loading

    The water cooling flange on the left side between the heater and furnace is used for pre-heated gas input and sealing

    Four-channel gas inlet (1/8" Dia tube and tube fitting) are built-in on the left side flange

    One small heater is attached to the left side flange of the furnace to preheat input gas, liquid, or evaporate solid chemical, which will be then delivered to the CVD furnace:

    Please click the picture left for more details:

    1.2''O.D x 6''L SS tube as the heating chamber

    Vacuum sealed 1" ID small quartz tube inside the heater

    400ºC Max. working temperature (1000ºC heater is available upon request)

    The flange on the left side is for gas sealing and input

    Rated Voltage

    Single Phase, 208-240 VAC, 50/60 Hz, AWG 8# Power cord is included (without plug)

    Power consumption

    Max. 3600 W (20 A breaker required)

    Heating Zone

    CVD Furnace:  440 mm

    Constant temperature zone: 100 mm 

    Gas Heater:     150mm

    Working Temperature

    CVD Furnace:

    Max heating temperature: 1100°C (< 2 hour)

    Continuous working temperature: 200~1000°C

    Max heating & cooling rate: 20°C/min

    Heater:

    Continuous working temperature: RT~600°C

    Max heating & cooling rate: 20°C/min

    Temperature Control

    CVD Furnace and Heater (separate temp control):

    Digital controllers with PID/self-tuning functions and 30 segments programmable

    Thermocouple: K-type thermocouples, at the right side flange through feedthrough to control furnace temperature.

    Control accuracy: +/- 1°C

    RS485 Communications Port

    Vacuum

    and Gas Sealing & Flange

    The right flange of the CVD furnace

    Water cooling flanges to prevent sealing o-ring from melting

    KF25 vacuum port to a pump

    Slidable for the customer to easily and fast push/pull in/out a sample

    One quartz wafer holder (3" Dia) is included and the flange with heating radiation block

    An anti-corrosive capacitance diaphragm gauge is included

    Left flange (between CVD Furnace and Heater) with four 1/8'' Swagelok fittings for 1/8'' tube:

    Two 1/8'' fitting on the flange for independently and directly delivering any gas into the CVD furnace

    One 1/8'' fitting for delivering heated gas from heater to CVD furnace

    One 1/4'' fitting for bypassing the gas (without heating) to the CVD furnace (inside the CVD furnace, the gas tube is merged with the heated gas pipe by a T fitting)

    Note: How gas pipe assembled in the CVD furnace through above 1/8'' fitting:

    One 1/4'' quartz tube delivers the vapor gas from the heater (also the bypass gas by a T fitting)

    Two 1/4'' quartz tube delivery extra gas via the two separate 1/8'' fitting on the big furnace left the flange

    These three 1/4'' quartz tubes inside the CVD furnace are in parallel and vertically 1'' higher than the sample holder

    These three 1/4'' quartz tubes can be easily removed to clean or replaced once get stuck or corroded

    The optional Liquid Injection device-optional

    For direct liquid CVD  ( DLCVD), you may consider the below devices for liquid injection:

    Net weight

    110kg

    Dimensions

    Standard:    62"L X 18"W X 23"H

    Maximum:   80"L X 18"W X 32"H  (Lid open and right-side flange slide out)

    Shipping Weight & Dimensions

    380 lbs

    48"x40"x54"

    Warranty

    One-year limited warranty for electrical parts. (Consumable parts such as processing tubes, o-rings and etc are not covered by the warranty)

    You may order a replacement quartz tube here:

    Laptop, software & WiFi Control (Optional)

    Brand new laptop with Microsoft Windows 10 

    Labview Based Temperature Control System enables the user to edit temperature profiles, manage heat-treatment recipes, record, and plot data for MTI furnaces.

    A wireless remote control provides up to 300 meters of operating range.

    Eurotherm temperature controller with software is available upon request at extra cost, which can provide +/- 0.1oC accuracy. ( see product options bar)

    Warning

    The tube furnaces with quartz tubes are designed for use under vacuum and low pressure <0.2 bars (relative to 1 atm, absolute pressure = 1.2 bar if used in air)

    Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. 

    Vacuum pressures may only be safely used up to 1000°C 

     

    CVD Chemical Vapor Deposition furnaces is a process which allows the creation of a deposit on the surface of mechanical parts, to protect them from oxidation and corrosion.